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Title
2-D NMR Developments Improve Monoclonal Antibody Characterization
Monday, September 26, 2016
Kimberly L. Colson
Ten years ago, industry commentators noted the increasing importance of biologics, and monoclonal antibodies (mAbs), in particular.
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Best Practices for CO
2
Incubator Maintenance
Friday, July 22, 2016
Mary Kay Bates
The use of long-established mutant lines in culture has shifted, and it is common to find researchers using more sensitive stem cells, primary cells and 3-D cultures in applications including vaccine...
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Quantitative Nanoparticle Analysis Based on Resistive Pulse Sensing
Friday, June 24, 2016
Andrew N. Cleland
Jean-Luc Fraikin
Peter Meinhold
Franklin Monzon
Nanoparticle analysis is becoming a central part of pharmaceutical development.
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Determination of Water Content and Dynamic Vapor Sorption Using Gravimetric Methods, Karl Fischer Titration and Thermal Analysis
Monday, June 20, 2016
Matthias Wagner
Virtually all materials interact with water. Accurate determination of a product’s water content and mechanism of water–solid interactions is required to define suitable processing, packaging, storage...
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SEMs Provide Deep Insight Into Materials
Wednesday, February 10, 2016
Donna Guarrera
Modern scanning electron microscopes (SEMs) offer vast improvements over early models in terms of electron optics, detector design and computing technology.
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Simplified Bioanalytical Sample Preparation
Wednesday, April 08, 2015
Erica Pike
The complexity of biological samples can pose challenges to downstream analysis in the pharmaceutical industry. Bioanalytical and drug metabolism and pharmacokinetics (DMPK) groups often work with ...
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Use of Microcalorimetry to Study Protein Stability
Monday, February 16, 2015
Rémi André
Link Brown
Differential scanning calorimetry (DSC) is used in the pharmaceutical, polymer and biotechnology industries to study the effect of temperature on a variety of solids or liquids, including those that ...
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Analytical Method Development in the Quality by Design Framework
Tuesday, December 16, 2014
Torgny Fornstedt
Dennis Åsberg
Jörgen Samuelsson
Anders Karlsson
Krzysztof Kaczmarski
The development of analytical methods in the Quality by Design (QbD) framework is currently gaining great momentum in the pharmaceutical industry. Presented here is a case study in which a ...
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Electrochemical Determination of Acetaminophen Using Gold Nanoparticles–Multiwall Carbon Nanotubes Modified Glassy Carbon Electrode
Monday, December 15, 2014
Youyuan Peng
Zhifu Zheng
Since their discovery in 1991, carbon nanotubes (CNTs) have been extensively studied for use in emitting devices, energy storage, sensor field, and biological and biomedical applications.
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Top Considerations When Automating Your Real-Time PCR Workflow
Thursday, October 16, 2014
Jennifer Reed
Kim Petro
With the increasing importance of large-scale data generation, many pharmaceutical labs are using robots to speed data collection. One such strategy is to automate the real-time PCR workflow.
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Thorough Risk Assessment Supports At-Scale Process Safety
Wednesday, July 16, 2014
Urs Groth
It goes without saying that in any manufacturing environment no one sets out to design an unsafe process. However, it is not enough to ensure a process will be safe under normal operating conditions.
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Improving the Crystallization Process for Optimal Drug Development
Friday, March 28, 2014
Michael Collazo
Soheila Vaezeslami
Sarah Burl
Macromolecular X-ray crystallography is an important and powerful technique in drug discovery. Studying the specific interactions of a particular drug with its protein target at the atomic level can ...
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Validation of Metal Impurities in Drug Products
Thursday, November 07, 2013
Alan Cross
The Elemental Impurities Chapters <232> and <233> were due to appear this year in the U.S. Pharmacopeia (with similar sections in the European Pharmacopeia). The date has now been pushed back pending the 233>232>...
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Automatic Motorized Leveling of Laboratory Balances
Friday, October 04, 2013
Thomas Pertsch
A fundamental rule for using high-resolution balances in pharmaceutical laboratories is that the instrument be level at all times. If the lab balance is not level, it cannot accurately measure objects...
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A Novel Sample Preparation Method for Complete Digestion of Complex Pharmaceutical Matrices
Friday, June 07, 2013
Reynhardt Klopper
Eric Fox
For more than 100 years, the USP General Chapter <231> concomitant visual test was the standard method for the determination and quantification of heavy metal impurities present in pharmaceutical products 231>...
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Understanding Concentration and Evaporation Technology: Part 2: Latest Developments in System Technology
Tuesday, February 26, 2013
Induka Abeysena
Rob Darrington
An understanding of the evaporative process and factors affecting it, involving careful selection of a vacuum pump, cold trap or condenser, and consideration of pressure control, is key to obtaining a...
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Understanding Concentration and Evaporation and Technology: Part 1: Basic Principles of Commonly Used Evaporation Techniques
Wednesday, February 06, 2013
Induka Abeysena
Rob Darrington
Solvent removal is an essential process across a broad range of applications in the pharmaceutical, chemical, and biotechnology industries. Although a diversity of sample formats and solvents are used...
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Second-Generation Expanded Bed Adsorption Scales from Lab to Plant
Thursday, January 17, 2013
Robert L. Stevenson, Ph.D.
Expanded bed adsorption (EBA) was introduced in 1999 with adsorbents that were used for pressure-driven packed beds. These had densities in the range of 1.1–1.5 g/mL, which was not much higher than ...
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