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A Convenient Sample Introduction System for ICP, ICP-MS, and AA
Sunday, October 01, 2006
Sample introduction has been a problem for analytical chemists for decades. In 1984, Richard Browner and Andrew Boorn went so far as to call sample introduction "The Achilles’ Heel of Atomic ...
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Statistics in Analytical Chemistry: Part 23—Degrees of Freedom in the Lack-of-Fit Test
Sunday, October 01, 2006
In the previous article (Part 22, American Laboratory, June/July 2006), the details behind the lack-of-fit (LOF) test were discussed.
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Nitrogen Generation in an Environmental Testing Laboratory
Thursday, September 07, 2006
Belmont Labs, located in Englewood, OH, is an environmental testing facility offering analytical services to clients in industry, civil/environmental engineering, and state and local governments.
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Peptide De Novo Sequencing With MALDI TOF/TOF: A Simple Approach Using Sulfonation Chemistry
Thursday, September 07, 2006
One of the main focuses of the scientific community, now that major advances have been achieved in the comprehension of genome organization, has become the study of proteins, including their structure...
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Rapid Screening of Complex Mixtures by Thin Layer Chromatography–Bioluminescence
Friday, September 01, 2006
The screening of complex mixtures such as foodstuffs, beverages, dietary supplements, and wastewater for toxins and adulterants or potential biological activity is often expensive and time consuming.
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Is This Surface Clean? Cleaning Validation by Direct Spectroscopic Surface Analysis
Friday, September 01, 2006
Pharmaceutical manufacturers and formulators must be able to confirm that the equipment they use is clean before it is utilized.
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Saving Money on TOC Analyzer Gas Costs
Friday, September 01, 2006
Total organic carbon analyzers are increasingly popular as an accurate and inexpensive way to test for inorganic and organic carbon contamination in water samples.
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A Valve Switching Ion Chromatography System With Integrated Automation Management
Friday, September 01, 2006
Valve switching applications are becoming popular in ion chromatography (IC). Example applications include matrix diversion or matrix elimination prior to analysis of trace components.
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The Determination of Perchlorate in Water Using LC-MS-MS
Friday, September 01, 2006
Perchlorate is both a naturally occurring chemical and a man-made inorganic ion.
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Expanding the Limits of Closed- Vessel Microwave Sample Preparation
Thursday, August 10, 2006
Analytical chemists have long known that closed-vessel microwave sample preparation techniques are the most reliable way to achieve high-quality digestions—i.e., clear, precipitate-free solutions...
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Evaluation of the Accuracy and Reproducibility of a High-Temperature Differential Scanning Calorimeter by Heat Capacity Measurements
Tuesday, August 01, 2006
Differential scanning calorimetry (DSC) is used to determine thermodynamic properties including specific heat, glass transition, and melting points of a variety of materials. The need for accurate ...
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Breakthrough Technology for Bottom-Up Proteomics and Small Molecule Research
Tuesday, August 01, 2006
High mass resolution is a prerequisite for high mass accuracy. Both are key for the analysis of unknown samples. High resolution enables the separation and detection of isobaric signals that are ...
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Pressure Digestion or Microwave Pressure Digestion for Sample Preparation?
Tuesday, August 01, 2006
Element determination in solids is a multiple-stage process comprising sampling, mechanical sample preparation, and acid digestion procedures that completely convert the analytical materials into ...
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Design Strategies for Hyper-Clean Laboratories
Tuesday, August 01, 2006
Nanotechnology has been aptly described as the science of building a structure one atom at a time.
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Microfiltration Technology: A Sensible Approach to Automating Sample Preparation
Tuesday, August 01, 2006
In the world of laboratories, the discerning eye of an efficiency expert must wince while witnessing sample preparation.
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